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ChemicalBook CAS DataBase List Lithium deuteride
13587-16-1

Lithium deuteride synthesis

1synthesis methods
Lithium deuteride has been prepared by the direct combination of lithium and deuterium at 700°, the deuterium having been obtained from the oxide by the use of magnesium.
The laboratory preparation of lithium deuteride and lithium aluminium deuteride
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Yield:-

Reaction Conditions:

in neat (no solvent, gas phase);LiD produced in an IR abs. cell (stainless steel, ca 1000K) by react. of D2 gas with Li vapor; Li vapor pressure : ca 1 Torr, slow D2 gas flow: ca 0.5 and 1 Torr; LiD detected by IR diode laser spectroscopy;

References:

Yamada, Chikashi;Hirota, Eizi [Journal of Chemical Physics,1988,vol. 88,# 11,p. 6702 - 6706]

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