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3709-21-5

LABOTEST-BB LT00408946 synthesis

6synthesis methods
-

Yield:3709-21-5 100%

Reaction Conditions:

Stage #1: ethyl 2-(ethoxycarbonyl)-4-phenylbutanoatewith water;sodium hydroxide in tetrahydrofuran;methanol; for 0.5 h;Reflux;
Stage #2: with hydrogenchloride in tetrahydrofuran;methanol;water; pH=< 1;

References:

Orrling, Kristina M.;Marzahn, Melissa R.;Gutierrez-de-Teran, Hugo;Aqvist, Johan;Dunn, Ben M.;Larhed, Mats [Bioorganic and Medicinal Chemistry,2009,vol. 17,# 16,p. 5933 - 5949] Location in patent:experimental part

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