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ChemicalBook CAS DataBase List L-A-GLYCERYLPHOSPHORYLCHOLINE(GPC)
4217-84-9

L-A-GLYCERYLPHOSPHORYLCHOLINE(GPC) synthesis

3synthesis methods
Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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Yield: 97%

Reaction Conditions:

with IONAC NM60 SG ion exchange resin in water

Steps:

3
Example 3: Preparation of L-oglycerophosphorylcholine (1)52.08g of L-α-glycerophosphorylcholine chloride obtained in the above Example2 was dissolved in purified water, and passed through IONAC NM60 SG ion exchange resin (Bayer). 0.1N silver nitrate was used to confirm the elimination of chloride ion.L-α-glycerophosphorylcholine which is the final product was obtained by decompressed concentration of the resultant (49.45g, yield 97%). 1H NMR (D2O, 300MHz): δ 3.21 (s, 9H), 3.63 (m, 4H), 3.90 (m, 4H), 4.30 (m, 2H). 13C NMR (D2O, 100MHz): δ 53.87, 59.35, 61.90, 65.93, 66.45, 70.53

References:

KIM, Hyun Joo WO2007/145476, 2007, A1 Location in patent:Page/Page column 10-11