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ChemicalBook CAS DataBase List L-2-Amino-3-ethylpentanoic acid
14328-49-5

L-2-Amino-3-ethylpentanoic acid synthesis

6synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: methanol; water
2.1: sulfuric acid
3.1: palladium on activated charcoal; hydrogen / methanol / 48 h / 20 °C / 3102.97 Torr
4.1: hydrogenchloride / water / 24 h / Reflux
4.2: solid-phase extraction column, C18-E, 55 μm, 70 ?,Phenomenex, Torrance, CA

References:

Sorbara, Noa T.;MacMillan, Joshua W. M.;McCluskey, Gregory D.;Bearne, Stephen L. [Organic and Biomolecular Chemistry,2019,vol. 17,# 37,p. 8618 - 8627]