ISOBUTYL LACTATE synthesis
- Product Name:ISOBUTYL LACTATE
- CAS Number:585-24-0
- Molecular formula:C7H14O3
- Molecular Weight:146.18
Yield:-
Reaction Conditions:
with tin-titanium-silicon molecular sieve at 60; for 7 h;
Steps:
4 Example 4
Weigh 0.15g of the tin-titanium-silicon molecular sieve Sn-Ti-MFI-4 provided in Preparation Example 4 as a catalyst and put it in a 15mL glass reaction tube, then add a magnetic stirrer, 8g isobutanol, and 0.1g pyruvaldehyde in sequence, and screw on Glass reaction tube lid. Put the glass reaction tube in the oil bath on the temperature-controlled magnetic stirrer, start the magnetic stirrer and heating device, and start the reaction. The reaction temperature was controlled at about 60°C and reacted for 7 hours. The specific reaction results are shown in Table 1.
References:
Sinopec Corporation;Sinopec Corporation Petrochemical Sciences Institute;Liu Yujia;Xia Changjiu;Zhao Yi;Peng Xinxin;Yang Yongjia;Lin Min;Zhu Bin;Luo Yibin;Shu Xingtian CN111253248, 2020, A Location in patent:Paragraph 0193; 0194; 0210