hypoglycin synthesis
- Product Name:hypoglycin
- CAS Number:156-56-9
- Molecular formula:C7H11NO2
- Molecular Weight:141.17
139242-82-3
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: 65 percent / pyridine, p-toluenesulfonyl chloride / CCl4; diethyl ether / 21 h / Ambient temperature; 1.) 0 deg C
2: 90 percent / n-BuLi / tetrahydrofuran; hexane / -78 deg C, 2 h 25 min, then room temp., 2 h 25 min
3: 0.25M HCl / H2O / 70 h / Ambient temperature
4: LiOH*H2O / tetrahydrofuran; H2O / 24 h / Ambient temperature
References:
Baldwin, Jack E.;Adlington, Robert M.;Bebbington, David;Russell, Andrew T. [Tetrahedron,1994,vol. 50,# 41,p. 12015 - 12028]
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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156-56-9
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1000210-73-0
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156-56-9
17 suppliers
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1000210-73-0
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156-56-9
17 suppliers
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