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ChemicalBook CAS DataBase List 2-Pyridinecarboxylic acid, 4-methyl-, hydrochloride (1:1)
123811-73-4

2-Pyridinecarboxylic acid, 4-methyl-, hydrochloride (1:1) synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: dimethylcarbamyl chloride / CH2Cl2 / 24 h / Ambient temperature
2: 93 percent / 6 N HCl / 24 h / Heating

References:

Shuman, Robert T.;Ornstein, Paul L.;Paschal, Jonathan W.;Gesellchen, Paul D. [Journal of Organic Chemistry,1990,vol. 55,# 2,p. 738 - 741]