Guaiacol synthesis
- Product Name:Guaiacol
- CAS Number:90-05-1
- Molecular formula:C7H8O2
- Molecular Weight:124.14
5720-06-9
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$5.00/1g
90-05-1
756 suppliers
$5.00/1g
Yield:90-05-1 99%
Reaction Conditions:
with hydrazine hydrate;caesium carbonate at 80; for 8 h;
Steps:
2 Example 2 Compound 2:
25 mL of the reaction flask was added hydrazine hydrate (0.25 mmol)2-methoxyphenylboronic acid (0.5 mmol),Cesium carbonate (1.0 mmol)And polyethylene glycol-400 (2.0 g).The mixture was reacted at 80 ° C until the reaction was complete.The reaction mixture was cooled to room temperature and the solvent was evaporated under reduced pressure. The product was separated by column chromatography to yield 99% yield.
References:
CN103936538,2017,B Location in patent:Paragraph 0027; 0031; 0032
529-28-2
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90-05-1
756 suppliers
$5.00/1g
578-57-4
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90-05-1
756 suppliers
$5.00/1g