FMOC-L-Methionine synthesis
- Product Name:FMOC-L-Methionine
- CAS Number:71989-28-1
- Molecular formula:C20H21NO4S
- Molecular Weight:371.45
63-68-3
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82911-69-1
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71989-28-1
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Yield:71989-28-1 78%
Reaction Conditions:
with sodium hydrogencarbonate in N,N-dimethyl-formamide at 50;
Steps:
S101 Synthesis of Fmoc-methionin
Synthesis of Fmoc-methionine; 6 mmol methionine and6.3 mmol of Fmoc-OSu was added to 20 ml of DMF (N, N-dimethylformamide)Subsequently, 6.3 mmol of NaHCO3 was added to remove the solvent and the remaining amine compound, which was then purified at 50CDried overnight in an empty oven to give 78% product yield;
References:
Southwest Petroleum University;He, Yi;Yang, Ranran;Zhou, Yanqiu;Fan, Yi;Qing, Dayong;Ma, Lan;Zhan, Yingqing;Chen, Zhao CN105622471, 2016, A Location in patent:Paragraph 0019; 0020
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28920-43-6
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71989-28-1
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1131148-55-4
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71989-28-1
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71989-28-1
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71989-28-1
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$6.41/1 mmol