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ChemicalBook CAS DataBase List FMOC-L-2-PYRIDYLALANINE
185379-40-2

FMOC-L-2-PYRIDYLALANINE synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: 94 percent / pyridine
2.1: 92 percent / NaI / acetone / 20 °C
3.1: Zn; 1,2-dibromoethane; Me3SiCl / dimethylformamide / 2 h / 35 °C
3.2: 57 percent / Pd(PPh3)2Cl2 / dimethylformamide
4.1: 60 percent / aq. LiOH / tetrahydrofuran / 20 °C

References:

Tabanella, Stefania;Valancogne, Ingrid;Jackson, Richard F W [Organic and biomolecular chemistry,2003,vol. 1,# 23,p. 4254 - 4261]

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