ETHYL TRANS-4-DECENOATE synthesis
- Product Name:ETHYL TRANS-4-DECENOATE
- CAS Number:76649-16-6
- Molecular formula:C12H22O2
- Molecular Weight:198.3
3391-86-4
430 suppliers
$10.00/1g
78-39-7
362 suppliers
$9.00/1g
76649-16-6
83 suppliers
$32.00/10mL
Yield:76649-16-6 99.9%
Reaction Conditions:
with propionic acid at 150; for 3 h;Claisen Rearrangement;Temperature;
Steps:
2.1 (1) Preparation of ethyl 4-decenoate
12.82 g of 1-octen-3-ol and 64.90 g of triethyl orthoacetate,Propionic acid 0.44g,Heated to 150 ,While distilling off the generated ethanol,The reaction was completed for about 3 hours.Excess distilled triethyl orthoacetate was distilled off under reduced pressure.Then use the oil pump distillation to get liquidEthyl 4-decenoate19.86g,Yield 99.9%.
References:
Beijing Liyuan Xin Sai Chemical Co., Ltd.;Jia Yanyong CN106748641, 2017, A Location in patent:Paragraph 0021; 0023; 0025
592-76-7
120 suppliers
$25.10/u
29493-00-3
2 suppliers
inquiry
74-85-1
106 suppliers
$79.00/11l
76649-16-6
83 suppliers
$32.00/10mL
14277-17-9
0 suppliers
inquiry
3391-86-4
430 suppliers
$10.00/1g
802294-64-0
1 suppliers
inquiry
78-39-7
362 suppliers
$9.00/1g
76649-16-6
83 suppliers
$32.00/10mL
592-76-7
120 suppliers
$25.10/u
1968-40-7
89 suppliers
$27.89/1g
29493-00-3
2 suppliers
inquiry
74-85-1
106 suppliers
$79.00/11l
76649-16-6
83 suppliers
$32.00/10mL
14277-17-9
0 suppliers
inquiry
592-76-7
120 suppliers
$25.10/u
1968-40-7
89 suppliers
$27.89/1g
7206-17-9
1 suppliers
inquiry
76649-16-6
83 suppliers
$32.00/10mL
14277-17-9
0 suppliers
inquiry