ETHYL 4-PHENYLPYRROLE-3-CARBOXYLATE synthesis
- Product Name:ETHYL 4-PHENYLPYRROLE-3-CARBOXYLATE
- CAS Number:64276-62-6
- Molecular formula:C13H13NO2
- Molecular Weight:215.25
17282-40-5
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100-52-7
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64276-62-6
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$58.00/1g
Yield:64276-62-6 96%
Reaction Conditions:
with sodium azide;L-valine at 20;Reagent/catalyst;
Steps:
1
ethyl α-bromoacetate (200mg, 1.2mmol) and pyridine (138mg, 1.8mmol) was dissolved in DMSO (5mL), stirred at room temperature for 5 hours. Then benzaldehyde (191 mg, 1.8 mmol), NaN3 (117 mg, 1.8 mmol) and L-valine were added.(14 mg, 0.12 mmol), the reaction was stirred at room temperature. After completion of the reaction, the reaction solution was poured into ice water and extracted with ethyl acetate (20 mL × 4).
References:
CN108358859,2018,A Location in patent:Paragraph 0021-0032
103-36-6
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36635-61-7
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64276-62-6
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$58.00/1g
4192-77-2
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64276-62-6
44 suppliers
$58.00/1g
36635-61-7
506 suppliers
$5.00/5g
4192-77-2
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$11.00/25g
64276-62-6
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$58.00/1g
867-13-0
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![Benzene, 1-[(isocyanatomethyl)sulfonyl]-4-methyl-](/CAS/20180601/GIF/10564-55-3.gif)
10564-55-3
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100-52-7
953 suppliers
$21.30/2g
64276-62-6
44 suppliers
$58.00/1g