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ChemicalBook CAS DataBase List ETHYL 3,5-DIMETHYLISOXAZOLE-4-CARBOXYLATE
17147-42-1

ETHYL 3,5-DIMETHYLISOXAZOLE-4-CARBOXYLATE synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: toluene / 1 h / Dean-Stark; Reflux; Inert atmosphere
2: triethylamine; trichlorophosphate / chloroform / 0.17 h / Inert atmosphere; Cooling with ice

References:

Qiu, Rongmao;Luo, Guoshun;Li, Xinyu;Zheng, Fan;Li, Haolin;Zhang, Jin;You, Qidong;Xiang, Hua [Bioorganic and Medicinal Chemistry Letters,2018,vol. 28,# 17,p. 2879 - 2884]

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