ETHYL (2E)-CHLORO(PHENYLHYDRAZONO)ACETATE synthesis
- Product Name:ETHYL (2E)-CHLORO(PHENYLHYDRAZONO)ACETATE
- CAS Number:28663-68-5
- Molecular formula:C10H11ClN2O2
- Molecular Weight:226.66
62-53-3
679 suppliers
$10.00/1g
609-15-4
458 suppliers
$6.00/25g
28663-68-5
56 suppliers
$40.00/500mg
Yield:28663-68-5 95%
Reaction Conditions:
Stage #1: aniline;ethyl 2-chloro-3-oxo-butyratewith hydrogenchloride;sodium nitrite in ethanol;water at -5 - 5;
Stage #2: ethyl 2-chloro-3-oxo-butyratewith sodium acetate in ethanol;water at -5; for 4 h;
References:
Yang, Wei;Li, Yingjun;Ai, Yong;Obianom, Obinna N.;Guo, Dong;Yang, Hong;Sakamuru, Srilatha;Xia, Menghang;Shu, Yan;Xue, Fengtian [Journal of Medicinal Chemistry,2019,vol. 62,# 24,p. 11151 - 11164]
100-63-0
384 suppliers
$10.00/1g
609-15-4
458 suppliers
$6.00/25g
28663-68-5
56 suppliers
$40.00/500mg
80447-71-8
0 suppliers
inquiry
28663-68-5
56 suppliers
$40.00/500mg
35157-75-6
1 suppliers
inquiry
28663-68-5
56 suppliers
$40.00/500mg
100-63-0
384 suppliers
$10.00/1g
28663-68-5
56 suppliers
$40.00/500mg