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1173023-24-9

(DTBM)2PH synthesis

3synthesis methods
535925-40-7 Synthesis
(DTBM)2P(O)H

535925-40-7
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Yield:1173023-24-9 60%

Reaction Conditions:

with lithium aluminium tetrahydride in diethyl ether;Reflux;

References:

Ganss, Stephanie;Breit, Bernhard [Angewandte Chemie - International Edition,2016,vol. 55,# 33,p. 9738 - 9742][Angew. Chem.,2016,vol. 128,# 33,p. 9890 - 9894,5] Location in patent:supporting information