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ChemicalBook CAS DataBase List DICHLOROETHOXYOXOVANADIUM (V)
1801-77-0

DICHLOROETHOXYOXOVANADIUM (V) synthesis

4synthesis methods
-

Yield:1801-77-0 97%

Reaction Conditions:

in dichloromethane;byproducts: (CH3)3SiCl; (N2); addn. of 2 equiv. of silane deriv. to CH2Cl2 soln. of vanadium compd. at room temp., stirring for 2 h at room temp.; evapn., elem. anal.;

References:

Romero-Fernandez, Javier;Carrillo-Hermosilla, Fernando;Antinolo, Antonio;Alonso-Moreno, Carlos;Rodriguez, Ana M.;Lopez-Solera, Isabel;Otero, Antonio [Dalton Transactions,2010,vol. 39,# 28,p. 6419 - 6425]