Dibenzo[b,mno]fluoranthene synthesis
- Product Name:Dibenzo[b,mno]fluoranthene
- CAS Number:668-30-4
- Molecular formula:C22H12
- Molecular Weight:276.33
68572-87-2
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: tetrakis-(triphenylphosphine)-palladium; caesium fluoride / 1,2-dimethoxyethane / 16 h / Reflux; Inert atmosphere
2: potassium carbonate / dichloromethane; methanol
3: γ-Al2O3 / 1,2-dichloro-benzene / 12 h / 190 °C / Microwave irradiation; Sealed tube
References:
Akhmetov, Vladimir;Feofanov, Mikhail;Ruppenstein, Cordula;Lange, Josefine;Sharapa, Dmitry;Krsti?, Marjan;Hampel, Frank;Kataev, Evgeny A.;Amsharov, Konstantin [Chemistry - A European Journal,2022,vol. 28,# 31,art. no. E202200584]
99134-25-5
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