Diaminomaleonitrile synthesis
- Product Name:Diaminomaleonitrile
- CAS Number:1187-42-4
- Molecular formula:C4H4N4
- Molecular Weight:108.1
75-86-5
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1187-42-4
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Yield:1187-42-4 88%
Reaction Conditions:
with sodium cyanide;methylthiol at 60; for 2 h;Autoclave;Temperature;Time;Reagent/catalyst;
Steps:
2
Example 2 In an autoclave, 10 g of NaCN is added to 130 ml of acetone cyanohydrin. Then 6.54 g of methanethiol is added. The solution is then stirred at 60° C. for 2 hours. The solution turns orange. The excess acetone cyanohydrin is then neutralized by adding soda. The solution is then filtered and evaporated to give an orange-yellow solid (amount recovered=33.7 g corresponding to a yield=88%).
References:
US2015/197487,2015,A1 Location in patent:Paragraph 0029
129694-52-6
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