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ChemicalBook CAS DataBase List Diallyl sulfide
592-88-1

Diallyl sulfide synthesis

12synthesis methods
From allyl iodide plus potassium sulfide in alcoho
-

Yield:592-88-1 90%

Reaction Conditions:

with iodine;sodium hydrogensulfite in chloroform at 50; for 3 h;Temperature;

Steps:

General procedure:
General procedure: A mixture of a sulfoxide (1 mmol), NaHSO3 (1.1 mmol), and I2 (0.025-0.1 mmol) in CHCl3 (1 mL) was stirred at room temperature or at 50 °C. The progress of the reaction was monitored by TLC. After completion, the solution was decanted from the residue, washed with EtOAc (2 x 1 mL). The combined organic layers were concentrated and the residue purified by chromatography on silica gel using n-hexane as eluent.

References:

Abbasi, Mohammad;Mohammadizadeh, Mohammad Reza;Moradi, Zahra [Tetrahedron Letters,2015,vol. 56,# 47,p. 6610 - 6613]

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