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ChemicalBook CAS DataBase List DELTA-NONANOLACTONE
6008-27-1

DELTA-NONANOLACTONE synthesis

11synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 82 percent / Et3N / CH2Cl2 / 2 h / 0 °C
2: 70 percent / CuCl*tris(pyridin-2-ylmethyl)amine complex / 1,2-dichloro-ethane / 80 °C
3: 92 percent / Bu3SnH; AIBN / cyclohexane / 3 h / 80 °C

References:

De Campo, Floryan;Lastecoueres, Dominique;Verlhac, Jean-Baptiste [Journal of the Chemical Society. Perkin Transactions 1 (2001),2000,# 4,p. 575 - 580]