CYCLO(-HIS-PHE) synthesis
- Product Name:CYCLO(-HIS-PHE)
- CAS Number:56586-95-9
- Molecular formula:C15H16N4O2
- Molecular Weight:284.31
13734-34-4
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20866-46-0
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56586-95-9
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Yield:56586-95-9 39%
Reaction Conditions:
Stage #1: N,1'-bis[(1,1-dimethylethoxy)carbonyl]-L-histidinewith triethylamine in N,N-dimethyl-formamide; for 24 h;
Stage #2: with hydrogenchloride in ethyl acetate; for 0.5 h;
Stage #3: N-tert-butoxycarbonyl-L-phenylalanineFurther stages;
References:
Kleinsmann, Alexander J.;Nachtsheim, Boris J. [Chemical Communications,2013,vol. 49,# 71,p. 7818 - 7820] Location in patent:supporting information
1161-13-3
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56586-95-9
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$147.00/50mg
2578-84-9
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56586-95-9
29 suppliers
$147.00/50mg
![L-Histidine, N-[(phenylmethoxy)carbonyl]-L-phenylalanyl-, methyl ester](/CAS/20210305/GIF/16689-13-7.gif)
16689-13-7
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56586-95-9
29 suppliers
$147.00/50mg
76524-86-2
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56586-95-9
29 suppliers
$147.00/50mg