Cyclamic acid synthesis

4synthesis methods

Product Name:Cyclamic acid
CAS Number:100-88-9
Molecular formula:C6H13NO3S
Molecular Weight:179.24

108-91-8 Synthesis

108-91-8
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100-88-9
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Yield:-

Reaction Conditions:

with chlorosulfonic acid in acetonitrile at 20; for 2 h;

Steps:

General procedure for synthesis of catalysts NSA 01-05, NSA 07 and NSA 08
General procedure: To a round-bottom flask containing nitrogenatedcompound (1 mmol, amine, urea or thiourea) in dry acetonitrile (3 mL), it was added chlorosulfonic acid (1 mmol) dropwise over a period of 20 min at room temperature. The reactional mixture was stirred for 2 h,and the acetonitrile was removed under vacuum to givethe catalysts.

References:

Hack, Carolina R. L.;Porciuncula, Larissa;Weber, Andressa C. H.;D’Oca, Caroline R. M.;Russowsky, Dennis;Moura, Jaqueline M.;Pinto, Luiz A. A.;D’Oca, Marcelo G. M. [Journal of the Brazilian Chemical Society,2018,vol. 29,# 11,p. 2342 - 2349]

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