ChemicalBook CAS DataBase List CAPRYLOHYDROXAMIC ACID

CAPRYLOHYDROXAMIC ACID synthesis

9synthesis methods

Product Name:CAPRYLOHYDROXAMIC ACID
CAS Number:7377-03-9
Molecular formula:C8H17NO2
Molecular Weight:159.23

124-07-2 Synthesis

124-07-2
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$6.00/25g

7377-03-9
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$5.00/5g

Yield:7377-03-9 95.81%

Reaction Conditions:

Stage #1: Octanoic acidwith acetic anhydride for 0.166667 h;
Stage #2: with hydroxylamine hydrochloride for 0.666667 h;

Steps:

5; 6 Example 5

29.13g n-octanoic acid (content 99%)And 21.05 g of acetic anhydride (content 97%) was added to the ball mill jar,Grinding for 10 min,Then add 14.11g hydroxylamine hydrochloride (content 98.5%),After continuing to grind for 40 minutes,Get a white solid product,It is the target collector product.After analysis and testing,The content of n-octyl hydroxydecanoic acid is 50.21%,Based on n-octanoic acidN-octyl hydroxamic acidThe yield was 95.81%.

References:

CN109761854,2019,A Location in patent:Paragraph 0076-0082

106-32-1 Synthesis