(-)-Camphanic acid chloride synthesis
- Product Name:(-)-Camphanic acid chloride
- CAS Number:39637-74-6
- Molecular formula:C10H13ClO3
- Molecular Weight:216.66
124-83-4
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: phosphorus pentachloride / Cooling with ice
1.2: 12 h / 125 °C
2.1: sulfuric acid / Reflux
2.2: 110 °C
3.1: thionyl chloride / Reflux
References:
Gerlach, Hans;Kappes, Dag;Boeckman, Robert K.;Maw, Graham N. [Organic Syntheses,1993,vol. 71,p. 48 - 48]