ChemicalBook CAS DataBase List C-(4-METHOXY-PHENYL)-C-PHENYL-METHYLAMINE

C-(4-METHOXY-PHENYL)-C-PHENYL-METHYLAMINE synthesis

9synthesis methods

Product Name:C-(4-METHOXY-PHENYL)-C-PHENYL-METHYLAMINE
CAS Number:2538-34-3
Molecular formula:C14H15NO
Molecular Weight:213.27

123-11-5 Synthesis

123-11-5
864 suppliers
$10.00/10g

100-58-3
187 suppliers
$18.00/10ml

C-(4-METHOXY-PHENYL)-C-PHENYL-METHYLAMINE

2538-34-3
25 suppliers
$65.00/50mg

Yield:2538-34-3 83%

Reaction Conditions:

Stage #1: 4-methoxy-benzaldehyde;phenylmagnesium bromidewith diphenyl phosphoryl azide in tetrahydrofuran;diethyl ether at 0 - 40; for 20 h;Schlenk technique;Inert atmosphere;
Stage #2: with lithium aluminium tetrahydride in tetrahydrofuran;diethyl ether at 0; for 1 h;Schlenk technique;Inert atmosphere;

References:

Goswami, Pratik P.;Suding, Victoria P.;Carlson, Angela S.;Topczewski, Joseph J. [European Journal of Organic Chemistry,2016,vol. 2016,# 28,p. 4805 - 4809] Location in patent:supporting information

100-66-3 Synthesis