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ChemicalBook CAS DataBase List BOC-MET-GLY-OH
23446-03-9

BOC-MET-GLY-OH synthesis

6synthesis methods
-

Yield:23446-03-9 87.2%

Reaction Conditions:

with methanol;sodium hydroxide at 20; for 3 h;

Steps:

5

General procedure: Compound 9a (2.6 g, 10 mmol) in 50 ml methanol was treatedwith 1 M NaOH (30 ml), and stirred for 3 h at room temperature.The solvent was evaporated in vacuum and the residue wasadjusted to PH 2-3 with 1 M HCl. The mixture was extracted 3times by EtOAc. The organic phase was dried over Na2SO4. Evaporationof EtOAc provided compound 10a. White solid: yield 92.4%,

References:

Zhang, Jian;Li, Xiaoyang;Jiang, Yuqi;Feng, Jinhong;Li, Xiaoguang;Zhang, Yingjie;Xu, Wenfang [Bioorganic and Medicinal Chemistry,2014,vol. 22,# 11,p. 3055 - 3064]

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