Boc-D-aspartinol 4-Benzyl Ester synthesis
- Product Name:Boc-D-aspartinol 4-Benzyl Ester
- CAS Number:182748-72-7
- Molecular formula:C16H23NO5
- Molecular Weight:309.36
51186-58-4
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182748-72-7
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Yield: 95%
Reaction Conditions:
Stage #1:4-benzyl Boc-D-aspartate with 4-methyl-morpholine;isobutyl chloroformate in 1,2-dimethoxyethane at -10; for 0.166667 h;
Stage #2: with sodium tetrahydroborate in 1,2-dimethoxyethane;water
References:
Bergman, Ylva;Ciampini, Marisa;Jalal, Sania;Lagiakos, Helen Rachel;Aguilar, Marie-Isabel;Perlmutter, Patrick [Tetrahedron Asymmetry,2008,vol. 19,# 24,p. 2861 - 2863] Location in patent:experimental part