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ChemicalBook CAS DataBase List BIS(TRIPHENYLPHOSPHINE)DICARBONYLNICKEL
13007-90-4

BIS(TRIPHENYLPHOSPHINE)DICARBONYLNICKEL synthesis

5synthesis methods
The preparative method of Bis(triphenylphosphine)dicarbonylnickel: by treating Tetracarbonylnickel with 2 equiv of Triphenylphosphine or by dissolving Dichlorobis(triphenylphosphine)nickel(II) in ethanol and treating it with CO in the presence of MeSNa. Purification: recrystallize from benzene.
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Yield: 60%

Reaction Conditions:

with carbon monoxide;tetrabutylammomium bromide;triphenylphosphine in pyridineElectrochem. Process; Ni-anode, CO 1 bar, 293 K, 30 mA, 6.8 V, 8 h;

References:

Grobe, Joseph;Schneider, Bernd Heinz [Zeitschrift fur Naturforschung, Teil B: Anorganische Chemie, Organische Chemie,1981,vol. 36,# 1,p. 8 - 13]

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