BIS(TRICYCLOHEXYLTIN) SULFIDE synthesis
- Product Name:BIS(TRICYCLOHEXYLTIN) SULFIDE
- CAS Number:13121-76-1
- Molecular formula:C36H66SSn2
- Molecular Weight:768.39
17356-08-0
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13121-70-5
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$49.00/100mg
13121-76-1
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31710-09-5
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Yield:31710-09-5 20% ，13121-76-1 50%
Reaction Conditions:
in melt;byproducts: NH3, H2O; under N2 stream, equimolar amt. of educts gradually heated to 180-200°C, then temp. retained at 130-140.degree for 4 h; crude product was refluxed in CHCl3, filtered off, filtrate concd., kept in ice cold water for 15 min, The ((C6H11)3Sn)2S filtered, elem. anal., filtrate concd., the (C6H11)3NCS recrystd. from petroleum ether;
References:
Awasthi;Bhattacharya;Verma [Journal of the Indian Chemical Society,1982,vol. 59,# 2,p. 264 - 268]
7783-06-4
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$158.00/25ml
13121-70-5
81 suppliers
$49.00/100mg
13121-76-1
10 suppliers
inquiry