BETA-(2-THIENYL)-DL-ALANINE synthesis
- Product Name:BETA-(2-THIENYL)-DL-ALANINE
- CAS Number:2021-58-1
- Molecular formula:C7H9NO2S
- Molecular Weight:171.22
98-03-3
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2021-58-1
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Yield:-
Steps:
Multi-step reaction with 6 steps
1.1: NaBH4 / methanol / 20 °C
2.1: SOCl2; benzotriazole / CH2Cl2
3.1: NaH / dimethylformamide; various solvent(s) / 0.5 h / 20 °C
3.2: 82 percent / dimethylformamide; various solvent(s) / 7 h / 20 - 60 °C
4.1: NaOH / methanol / 20 h / 20 °C
5.1: toluene / 2 h / Heating
6.1: 75 percent / aq. LiOH / 2.5 h / 60 °C
References:
Paizs, Csaba;Katona, Adrian;Retey, Janos [Chemistry - A European Journal,2006,vol. 12,# 10,p. 2739 - 2744]
765-50-4
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2021-58-1
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636-72-6
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2021-58-1
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2021-58-1
101 suppliers
$30.00/1G