Benzenepropanoyl chloride, 4-fluoro- synthesis
- Product Name:Benzenepropanoyl chloride, 4-fluoro-
- CAS Number:133188-66-6
- Molecular formula:C10H10ClFO
- Molecular Weight:200.64
1583-67-1
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3096-81-9
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Yield:3096-81-9 75.3 g (100%)
Reaction Conditions:
with dichloro sulfoxide
Steps:
13.c c)
c) Preparation of 7-Fluoro-1-tetralone A mixture of 4-(4-fluorophenyl)butyric acid (68.2 g, 0.37 mol) and thionyl chloride (155 g, 1.3 mol) was refluxed for 1.25 h. The mixture was concentrated in vacuo to give 75.3 g (100%) of 4-(4-fluorophenyl)butyryl chloride)
References:
US5872118,1999,A
51787-96-3
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3096-81-9
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462-06-6
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3096-81-9
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366-77-8
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3096-81-9
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