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ChemicalBook CAS DataBase List Amino-PEG8-azide
1333154-77-0

Amino-PEG8-azide synthesis

11synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: triethylamine / dichloromethane / 3.5 h / 0 - 20 °C
2: N,N-dimethyl-formamide / 15 h / 110 °C
3: hydrazine / ethanol / 3 h / 60 °C

References:

Goswami, Lalit N.;Houston, Zachary H.;Sarma, Saurav J.;Jalisatgi, Satish S.;Hawthorne, M. Frederick [Organic and Biomolecular Chemistry,2013,vol. 11,# 7,p. 1116 - 1126]

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