AMINO-(3,4,5-TRIMETHOXY-PHENYL)-ACETIC ACID synthesis
- Product Name:AMINO-(3,4,5-TRIMETHOXY-PHENYL)-ACETIC ACID
- CAS Number:86053-97-6
- Molecular formula:C11H15NO5
- Molecular Weight:241.24
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: Na2S2O5 / methanol; H2O / 2 h / 35 °C
2: 84 percent / aq. H2O2; K2CO3 / dimethylsulfoxide / 16.5 h / 21 - 35 °C
3: 92 percent / NaOH; H2O / various solvent(s) / 3.5 h / Heating
4: hydrazine hydrate; NaOH / Pd/C / H2O; various solvent(s) / 10 h / Heating
References:
Davies, Antony J.;Ashwood, Michael S.;Cottrell, Ian F. [Synthetic Communications,2000,vol. 30,# 6,p. 1095 - 1102]
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