AKIYAMA'S REAGENT synthesis
- Product Name:AKIYAMA'S REAGENT
- CAS Number:101046-20-2
- Molecular formula:C20H16N2O3
- Molecular Weight:332.35
41602-56-6
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Yield:-
Steps:
Multi-step reaction with 5 steps
1: 56 percent / KOH / ethanol / 7 h / Heating
2: 86 percent / CH3ONa / ethanol / 0.33 h / Heating
3: 81 percent / active carbon, FeCl3*6H2O, hydrazine / benzene; methanol / 7 h / Heating
4: 84 percent
5: 46 percent / AcONa / acetic anhydride / Heating
References:
Akiyama, Shuzo;Akimoto, Hiroyuki;Nakatsuji, Shin'ichi;Nakashima, Kenichiro [Bulletin of the Chemical Society of Japan,1985,vol. 58,# 8,p. 2192 - 2196]
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