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101046-20-2

AKIYAMA'S REAGENT synthesis

7synthesis methods
41602-56-6 Synthesis
4-(DIMETHYLAMINO)SALICYLALDEHYDE

41602-56-6
85 suppliers
$24.00/100mg

AKIYAMA'S REAGENT

101046-20-2
6 suppliers
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Yield:-

Steps:

Multi-step reaction with 5 steps
1: 56 percent / KOH / ethanol / 7 h / Heating
2: 86 percent / CH3ONa / ethanol / 0.33 h / Heating
3: 81 percent / active carbon, FeCl3*6H2O, hydrazine / benzene; methanol / 7 h / Heating
4: 84 percent
5: 46 percent / AcONa / acetic anhydride / Heating

References:

Akiyama, Shuzo;Akimoto, Hiroyuki;Nakatsuji, Shin'ichi;Nakashima, Kenichiro [Bulletin of the Chemical Society of Japan,1985,vol. 58,# 8,p. 2192 - 2196]

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