ADENYLYL(3'>5')CYTIDINE FREE ACID synthesis
- Product Name:ADENYLYL(3'>5')CYTIDINE FREE ACID
- CAS Number:2382-66-3
- Molecular formula:C19H25N8O11P
- Molecular Weight:572.42
69504-15-0
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: 1.) 2,4,6-collidine / 1.) THF, -78 deg C, 10 min, 2.) THF, -78 deg C, 15 min; 20 deg C, 30 min
2: 70 percent / 2 percent benzenesulfonic acid / CHCl3; methanol / 2 h / Ambient temperature
3: 1.) t-butylamine, 2.) methanolic ammonia, 3.) TBAF
References:
Ogilvie, Kelvin K.;Theriault, Nicole Y.;Seifert, Jan-Marcus;Pon, Richard T.;Nemer, Mona J. [Canadian Journal of Chemistry,1980,vol. 58,p. 2686 - 2693]
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