(9H-Fluoren-9-yl)MethOxy]Carbonyl D-Lys(Ac)-OH synthesis
- Product Name:(9H-Fluoren-9-yl)MethOxy]Carbonyl D-Lys(Ac)-OH
- CAS Number:320410-22-8
- Molecular formula:C23H26N2O5
- Molecular Weight:410.46
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Yield:320410-22-8 56%
Reaction Conditions:
Stage #1: Nε-acetyl-lysine;N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimidewith sodium carbonate in 1,4-dioxane;water at 20;
Stage #2: with hydrogenchloride;water at 0; pH=1;
References:
Jamonnak, Nuttara;Hirsch, Brett M.;Pang, Yi;Zheng, Weiping [Bioorganic Chemistry,2010,vol. 38,# 1,p. 17 - 25] Location in patent:experimental part