(-)-N,N-DICYCLOHEXYL-(1S)-ISOBORNEOL-10- SULFONAMIDE synthesis
- Product Name:(-)-N,N-DICYCLOHEXYL-(1S)-ISOBORNEOL-10- SULFONAMIDE
- CAS Number:99295-72-4
- Molecular formula:C22H39NO3S
- Molecular Weight:397.61
![Decanoic acid, 1-[[(dicyclohexylamino)sulfonyl]methyl]-7,7-dimethylbicyclo[2.2.1]hept-2-yl ester, (1R-exo)- (9CI)](/CAS/20210305/GIF/96864-09-4.gif)
96864-09-4
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99295-72-4
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: LDA / tetrahydrofuran / -78 °C
2: 2.) NEt3*HF / 1.) CH2Cl2, -15 deg C, 15 min, 20 deg C, 30 min; 2.) 20 deg C, 4 h
3: 100 percent / K2CO3 / methanol / 20 h / 20 °C
References:
Oppolzer, Wolfgang;Dudfield, Philip [Helvetica Chimica Acta,1985,vol. 68,p. 216 - 219]
![Bicyclo[2.2.1]heptane-1-methanesulfonamide, N,N-dicyclohexyl-7,7-dimethyl-2-[[1-[(trimethylsilyl)oxy]-1-decenyl]oxy]-, [1R-[1α,2β(E),4β]]- (9CI)](/CAS/20210305/GIF/104926-27-4.gif)
104926-27-4
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99295-72-4
8 suppliers
$226.00/1g