2-(N,N-DIMETHYLCARBOXAMIDO)PHENYLBORONIC ACID PINACOL ESTER synthesis
- Product Name:2-(N,N-DIMETHYLCARBOXAMIDO)PHENYLBORONIC ACID PINACOL ESTER
- CAS Number:956229-73-5
- Molecular formula:C15H22BNO3
- Molecular Weight:275.15
73183-34-3
581 suppliers
$6.00/5g
611-74-5
212 suppliers
$10.00/5g
956229-73-5
40 suppliers
$130.00/250mg
Yield:956229-73-5 82%
Reaction Conditions:
Stage #1: bis(pinacol)diboranewith 5-methyl-2-(thiophen-3-yl)pyridine;(1,5-cyclooctadiene)(methoxy)iridium(I) dimer in tetrahydrofuran at 20; for 0.0333333 h;Inert atmosphere;Glovebox;
Stage #2: N,N-dimethylbenzamide in tetrahydrofuran at 100; for 12 h;Inert atmosphere;Sealed tube;regioselective reaction;
References:
Chattopadhyay, Buddhadeb;Hassan, Mirja Md Mahamudul;Hoque, Md Emdadul [Journal of the American Chemical Society,2021,vol. 143,# 13,p. 5022 - 5037] Location in patent:supporting information
65-85-0
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956229-73-5
40 suppliers
$130.00/250mg
98-88-4
584 suppliers
$10.00/5g
956229-73-5
40 suppliers
$130.00/250mg
611-74-5
212 suppliers
$10.00/5g
25015-63-8
223 suppliers
$22.39/5G
956229-73-5
40 suppliers
$130.00/250mg
832114-07-5
45 suppliers
$25.00/250mg
400727-57-3
77 suppliers
$10.00/250mg
73183-34-3
581 suppliers
$6.00/5g
611-74-5
212 suppliers
$10.00/5g
956229-73-5
40 suppliers
$130.00/250mg
832114-07-5
45 suppliers
$25.00/250mg
400727-57-3
77 suppliers
$10.00/250mg