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1705-82-4

9(10H)-Anthracenone, 10-diazo- synthesis

4synthesis methods
-

Yield:1705-82-4 86 %Spectr. ,84-65-1 7%

Reaction Conditions:

with 15-crown-5;2-azido-1,3-dimethylimidazolinium chloride;triethylamine in tetrahydrofuran;acetonitrile at -20; for 0.166667 h;

References:

Kitamura, Mitsuru;Tashiro, Norifumi;Sakata, Rie;Okauchi, Tatsuo [Synlett,2010,# 16,p. 2503 - 2505] Location in patent:experimental part