9,10-DIHYDROXYSTEARIC ACID synthesis

6synthesis methods

Product Name:9,10-DIHYDROXYSTEARIC ACID
CAS Number:120-87-6
Molecular formula:C18H36O4
Molecular Weight:316.48

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Yield: 80.3%

Reaction Conditions:

with dihydrogen peroxide;Nafion-SAC₁₃ in water at 90; for 20 h;Conversion of starting material;

Steps:

24 Example 24
Nafion-SAC13 (1.50 g), a 30% aqueous hydrogen peroxide solution (4.0 mL, 40.6 mmol), and oleic acid (3.20 mL, 10.1 mmol) were mixed and stirred at 90C for 20 hours. After the reaction, the resultant mixture was treated in the same manner as Example 1 to obtain 2.57 g (8.11 mmol) of 9,10-dihydroxyoctadecanoic acid (80.3% yield).

References:

Japan Science and Technology Agency;National Institute of Advanced Industrial Science and Technology EP1477468, 2004, A1 Location in patent:Page 7