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ChemicalBook CAS DataBase List 3-(4-Methyl-1-piperazinylmethyl)benzeneboronic acid pinacol ester, 97%
883738-27-0

3-(4-Methyl-1-piperazinylmethyl)benzeneboronic acid pinacol ester, 97% synthesis

7synthesis methods
109-01-3 Synthesis
1-Methylpiperazine

109-01-3
666 suppliers
$5.00/5G

443776-76-9 Synthesis
(3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanol

443776-76-9
104 suppliers
$8.00/250mg

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Yield:883738-27-0 80%

Reaction Conditions:

with [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2;sodium carbonate;bis[2-(diphenylphosphino)phenyl] ether in 5,5-dimethyl-1,3-cyclohexadiene at 155; for 24 h;Inert atmosphere;Reflux;

References:

Ma, Winson M. J.;James, Tony D.;Williams, Jonathan M. J. [Organic Letters,2013,vol. 15,# 18,p. 4850 - 4853] Location in patent:supporting information

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