N-TRIFLUOROACETYL-L-G-GLUTAMYL-L-CYSTEINE DIMETHYL ESTER, (2-2') DISULPHIDE synthesis
- Product Name:N-TRIFLUOROACETYL-L-G-GLUTAMYL-L-CYSTEINE DIMETHYL ESTER, (2-2') DISULPHIDE
- CAS Number:84344-30-9
- Molecular formula:C24H32F6N4O12S2
- Molecular Weight:746.65
56-86-0
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: 55 percent
2: 0.03 h / Heating
3: thionyl chloride / diethyl ether; dimethylformamide / 2 h / 23 °C
4: 1.) triethylamine / 1.) THF, 23 deg C, 15 h
References:
Ellis, Frank;Mills, Lester S.;North, Peter C. [Tetrahedron Letters,1982,vol. 23,# 36,p. 3735 - 3736]
1535-57-5
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