8-METHYLDECANOIC ACID synthesis
- Product Name:8-METHYLDECANOIC ACID
- CAS Number:5601-60-5
- Molecular formula:C11H22O2
- Molecular Weight:186.29
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: 8.05 g / SnCl4 / CH2Cl2 / 2.5 h / 0 °C
2: 5.04 g / amalgamated zinc / acetic acid / 12 h / 20 °C
3: H2 / Raney-Ni / propan-2-ol / 48 h
4: 3.35 g / 3 M NaOH / methanol; dioxane
References:
Hedenstroem, Erik;Nguyen, Ba-Vu;Silks III, Louis A. [Tetrahedron Asymmetry,2002,vol. 13,# 8,p. 835 - 844]
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