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10336-29-5

8-Methyl-1-naphthalenemethanol synthesis

6synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: 85 percent / aq. H3PO4 / 1 h / Heating
2.1: Li; naphthalene / tetrahydrofuran / 7 h / -15 °C
2.2: 55 percent Spectr. / H2O / tetrahydrofuran / 0.25 h

References:

Azzena, Ugo;Demartis, Salvatore;Pilo, Luciano;Piras, Elisabetta [Tetrahedron,2000,vol. 56,# 42,p. 8375 - 8382]