1,4,8,11-TETRAAZACYCLOTETRADECANE-1,4,8,11-TETRAACETIC ACID TETRAHYDROCHLORIDE HYDRATE synthesis

1synthesis methods

Product Name:1,4,8,11-TETRAAZACYCLOTETRADECANE-1,4,8,11-TETRAACETIC ACID TETRAHYDROCHLORIDE HYDRATE
CAS Number:78668-42-5
Molecular formula:C18H44Cl4N4O12
Molecular Weight:650.37

295-37-4 Synthesis

Yield:-

Reaction Conditions:

with hydrogenchloride;potassium hydroxide1.) water, 20 deg C -> 80 deg C, pH=9-10, 24 h; 2.) 24 h, reflux;Yield given. Multistep reaction;

References:

Stetter, H.;Frank, W.;Mertens, R. [Tetrahedron,1981,vol. 37,p. 767 - 772]

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