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ChemicalBook CAS DataBase List 3-AMINO-8-BENZYL-8-AZABICYCLO[3.2.1]OCTANE (3-EXO)-
76272-36-1

3-AMINO-8-BENZYL-8-AZABICYCLO[3.2.1]OCTANE (3-EXO)- synthesis

10synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: hydrogenchloride; water / 1 h / Reflux
1.2: 6 h / 0 - 50 °C
1.3: pH 12
2.1: hydroxylamine hydrochloride; pyridine / ethanol / 18 h / Reflux
3.1: sodium; pentan-1-ol / 2 h / Reflux

References:

SHANGHAI TARGETDRUG CO., LTD.;SHANGHAI INSTITUTE OF MATERIA MEDICA, CHINESE ACADEMY OF SCIENCES US2011/251192, 2011, A1