4-Pyrimidinamine, 2,5-dichloro-N-[2-[(1-methylethyl)sulfonyl]phenyl]- synthesis
- Product Name:4-Pyrimidinamine, 2,5-dichloro-N-[2-[(1-methylethyl)sulfonyl]phenyl]-
- CAS Number:761440-16-8
- Molecular formula:C13H13Cl2N3O2S
- Molecular Weight:346.23
1493-27-2
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761440-16-8
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$9.00/250mg
Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 100 °C
2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 16 h / 20 °C
3.1: hydrogen / palladium 10% on activated carbon / methanol / 6 h
4.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / Cooling
4.2: 16 h / 20 °C
References:
WO2011/140338,2011,A1
70415-85-9
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761440-16-8
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70415-86-0
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$45.00/50mg
761440-16-8
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6397-33-7
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$21.00/1g
761440-16-8
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88-73-3
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761440-16-8
236 suppliers
$9.00/250mg