tert-Butyl 6-[O-(2-Bromoethyl)phosphoryl)hydroxyhexanoate synthesis
- Product Name:tert-Butyl 6-[O-(2-Bromoethyl)phosphoryl)hydroxyhexanoate
- CAS Number:73839-25-5
- Molecular formula:C12H24BrO6P
- Molecular Weight:375.19
4224-70-8
347 suppliers
$7.00/5g
73839-25-5
13 suppliers
$110.00/500mg
Yield:-
Steps:
Multi-step reaction with 3 steps
1: 93 percent / H2SO4 / CH2Cl2 / Ambient temperature
2: 1) sodium formate, 2) KOH / 1) DMF, a) 110 deg C, 4h, b) RT, 2 days, 2) H2O, 30-40 deg C, 4h
3: 1) triethylamine, 2) pyridine, H2O / 1) RT, 1h, 2) RT
References:
Spande, Thomas F. [Journal of Organic Chemistry,1980,vol. 45,# 15,p. 3081 - 3084]
65868-63-5
62 suppliers
$44.00/100mg
73839-25-5
13 suppliers
$110.00/500mg
4167-02-6
19 suppliers
$125.00/250mg
73839-20-0
56 suppliers
$140.00/1g
73839-25-5
13 suppliers
$110.00/500mg