7-BENZYLOXY-3,4-DIHYDRO-1H-NAPHTHALEN-2-ONE synthesis
- Product Name:7-BENZYLOXY-3,4-DIHYDRO-1H-NAPHTHALEN-2-ONE
- CAS Number:71048-42-5
- Molecular formula:C17H16O2
- Molecular Weight:252.31
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: aluminium; mercury(I) chloride / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere
1.2: -78 °C / Inert atmosphere
2.1: 2,6-dichloropyridine N-oxide; C33H54AuClP; sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate / 1,2-dichloro-ethane / 5 h / 50 °C
References:
Ling, Hui-Bo;Chen, Zi-Sheng;Yang, Fang;Xu, Bin;Gao, Jin-Ming;Ji, Kegong [Journal of Organic Chemistry,2017,vol. 82,# 13,p. 7070 - 7076]