(2S,2'S)-(-)-2-HYDROXYMETHYL-1-[(1-METHYLPYRROLIDIN-2-YL)-METHYL]-PYRROLIDINE synthesis

3synthesis methods

Product Name:(2S,2'S)-(-)-2-HYDROXYMETHYL-1-[(1-METHYLPYRROLIDIN-2-YL)-METHYL]-PYRROLIDINE
CAS Number:66283-23-6
Molecular formula:C11H22N2O
Molecular Weight:198.31

Preparative Method of (2S,2′S)-2-Hydroxymethyl-1-[(1-methylpyrrolidin-2-yl)methyl]pyrrolidine: reduction of N-[N(-benzyloxycarbonyl)prolyl]proline methyl ester with Lithium Aluminum Hydride affords the title reagent in 81% yield.

L-Proline, 1-[1-[(phenylmethoxy)carbonyl]-L-prolyl]-, methyl ester

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(2S,2'S)-(-)-2-HYDROXYMETHYL-1-[(1-METHYLPYRROLIDIN-2-YL)-METHYL]-PYRROLIDINE

66283-23-6
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Yield:66283-23-6 81%

Reaction Conditions:

with lithium aluminium tetrahydride in tetrahydrofuran; for 3 h;Heating;

References:

Mukaiyama, Teruaki [Tetrahedron,1981,vol. 37,# 23,p. 4111 - 4119]

147-85-3 Synthesis

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References

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66283-23-6
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References

(2S,2'S)-(-)-2-HYDROXYMETHYL-1-[(1-METHYLPYRROLIDIN-2-YL)-METHYL]-PYRROLIDINE Related Search:

Z-PRO-PRO-OH H-GLY-PRO-PRO-OH H-GLY-PRO-HYP-OH

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(2S,2'S)-(-)-2-HYDROXYMETHYL-1-[(1-METHYLPYRROLIDIN-2-YL)-METHYL]-PYRROLIDINE synthesis

(2S,2'S)-(-)-2-HYDROXYMETHYL-1-[(1-METHYLPYRROLIDIN-2-YL)-METHYL]-PYRROLIDINE Related Search: